Synthesis of sodium silicate solution using rice hull ash waste from a local salt refinery / (Record no. 23526)

MARC details
000 -LEADER
fixed length control field 02315nam a22001817a 4500
003 - CONTROL NUMBER IDENTIFIER
control field OSt
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20240910160813.0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 240910b |||||||| |||| 00| 0 eng d
040 ## - CATALOGING SOURCE
Original cataloging agency MMSU
Transcribing agency ULS
100 ## - MAIN ENTRY--PERSONAL NAME
Personal name Menor, Ben John L.
245 ## - TITLE STATEMENT
Title Synthesis of sodium silicate solution using rice hull ash waste from a local salt refinery /
Statement of responsibility, etc. Ben John L. Menor
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. City of Batac :
Name of publisher, distributor, etc. MMSU,
Date of publication, distribution, etc. 2024.
300 ## - PHYSICAL DESCRIPTION
Extent xiiii, 48 leaves :
Dimensions 29 cm.
500 ## - GENERAL NOTE
General note UTHESIS (Bachelor of Science in Ceramic Engineering)
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Bibliography : leaves 30-32
520 ## - SUMMARY, ETC.
Summary, etc. Sodium silicate solution (Na2SiO3) is commonly used in ceramics as deflocculant and as industrial additive across various industries. It is commercially prepared by mixing sand as silica (SiO2) source and sodium hydroxide (NaOH) or sodium carbonate as source of sodium oxide then heated to a very high temperature. This study, synthesized Na2SiO3 as SiO2 source (11.5 g) using waste rice hull ash (RHA), an agricultural waste with minimal value, from a local salt refinery, and commercial NaOH (60 mL, 1.5 M). The mixtures were reacted at low temperature (100 oC) at varying reaction times (1, 2, and 3 hours) labelled as 1 HRT, 2 HRT, and 3 HRT, respectively. Properties such as specific gravity, viscosity, pH, electrical conductivity, and as deflocculant in clay slurry of the as-synthesized and adjusted Na2SiO3 were evaluated. The chemical composition particularly the SiO2 percentage present in the collected and processed RHA as well the residue in the synthesis process were analyzed using XRF technique. Chemical analysis showed that the amount of SiO2 in RHA is 95.14 % while the residue in the synthesis still contains unreacted SiO2. In addition, the calculated SiO2/Na2O ratio of 1 HRT, 2 HRT, 3 HRT were 1.85, 2.09, and 2.34, respectively. The amount of SiO2 reacted increased with longer reaction time. Further, the viscosity and electrical conductivity decreased with longer reaction time. Moreover, results of the clay slurry deflocculation tests using the Na2SiO3 synthesized at different reaction time revealed that 2HRT and 3HRT are comparable to the commercial. These results validate the potential of waste RHA as source of SiO2 in producing valuable Na2SiO3 thereby, promoting waste valorization. <br/><br/>
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Source of classification or shelving scheme
Koha item type Thesis/Dissertation
Holdings
Withdrawn status Lost status Source of classification or shelving scheme Damaged status Not for loan Home library Current library Shelving location Date acquired Inventory number Total Checkouts Barcode Date last seen Price effective from Koha item type Public note
          MMSU Main Library MMSU Main Library Theses and Dissertation Section 09/10/2024 6940   UTHESIS-6940 09/10/2024 09/10/2024 Thesis/Dissertation Room Use Only

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